China 75932-02-4 N-α,N-ε-di-Fmoc-D-lysine Moetsi le Feme |Jiayinglai

75932-02-4 N-α,N-ε-di-Fmoc-D-lysine

Tlhaloso e Khutšoanyane:

Ponahalo	Phofo e tšoeu ho isa ho e tšoeu
MF	C36H34N2O6
MW	590.66
Bohloeki	98+

Re romelle lengolo-tsoibila

Lintlha tsa Sehlahisoa

Boemo ba lipalangoang&mokhoa oa ho romella o khothalelitsoeng:
ka moya, ka lewatle kapa ka polelo

Boemo ba polokelo:
2-8°C

Bonyane Bonyane ba Odara:
Puisano

Setifikeiti:
COA, HPLC, GC, HNMR, Assay, Water Content(KF), TLC e teng

Litlhaloso tse tšoanang

Na,Ne-di-Fmoc-D-lysine;

N-.ALPHA.,N-.EPSILON.-DI-FMOC-D-LYSINE;

(R) -1,13-di(9H-fluoren-9-yl)-3,11-dioxo-2,12-dioxa-4,10-diazatridecane-5-carboxylicacid;

D-Lysine,N2,N6-bis[(9H-fluoren-9-ylMethoxy)carbonyl]-;

FMoc-D-Ls(FMoc)-OHN-α,N-ε-di-FMoc-D-lysine;

N2,N6-Bis-FMoc-D-lysine;

N2,N6-Bis[(9H-fluoren-9-ylMethoxy)carbonyl]lysine

Ho paka ka hare

Hangata li sebelisoa ho paka phofo.'Me li ka thibela khanya ea letsatsi le metsi hore li se ke tsa senyeha.

ho phuthela ka ntle

Lebokose le thata le ka sireletsa lihlahisoa tsa hau ho senya le ho koloba.

Lisebelisoa

Li-amino acid tse sireletsang habeli haholo-holo li kenyelletsa D-lys-OH e nang le lihlopha tsa amino tse mahlakoreng le ketane e nang le ketane.pho potoloha ha L-Rag-OH.Bakeng sa sehlopha sa AA-amin, leano la tšireletso la FMOC le ntse le amoheloa, 'me malome oa bobeli oa carbonate tse peli o sebelisoa ketane ea mahlakoreng.Tibon e kenngoa sehlopheng sa liphaephe tsa oxygenyl ho sireletsa Fu Fu 5 ~ Sulfidal ho sireletsa.Hobane ho na le mehato e mengata ea ho kopanya li-amino acid tsena tse peli, karabelo ea mantlha karabong ea mantlhasteps etsa liteko tsa ho ntlafatsa ntho e le 'ngoe.Tšireletso ea D-LYS-OH haholo-holo e nahana ka nako e amang moloko oa koporo e lekanangthemocheso, le nako ea ho tlosa koporo.Tšireletso ea L-Rag-OH haholo-holo e nahana ka ho lokisetsa Z-RG-OH. Ka nako eo, mocheso oa ZL-Rag (PBF) -OH selikalikoe sa letsoai la ammonia, hammoho le palo ea li-catalyst ha hydrogen e entsoe ka Z,

Khatello, mocheso le nako ea karabelo li fumane tlhahiso e ntle ka liteko tsa ho ntlafatsa.

Nakong ea ts'ebetso ea karabelo, ts'ebetso ea ho lemoha ha T.C e amoheloa haholo-holo, 'me maemo a crystallization a sehlahisoa a ntlafatsoa.

Bohloeki ba sehlahisoa bo ne bo lekantsoe ka chromatography ea metsi e sebetsang hantle haholo, 'me bohloeki ba sehlahisoa bo fihlile ho feta 95.0%.Ho phaella ho matšoao a tloaelehileng a 'mele kamehla, hapeiho kenyeletsoa mabone a infrared, mass spectrum kapa hydrogen spectrum.

lihlahisoa tse amanang

L-Ls(Boc)	Lys(Fmoc)-OH	L-Ls(Cbz)-OH	D-Ls(Fmoc).HCl
Lys(Fmoc).HCl	Boc-Ls(Boc)-OH	Boc-L-Ls(Boc)-OH·DCHA	Boc-D-Ls(Boc)-OH
Boc-L-Ls(Fmoc)-OH	Fmoc-L-Ls(tfa)-OH	Fmoc-L-Ls(DDC)	Fmoc-L-Ls(Cbz)
Fmoc-L-Ls(AC)	Fmoc-L-Ls(Fmoc)-OH	Fmoc-D-Ls(Boc)-OH	Fmoc-L-Ls(Boc)-OH
Cbz-L-Lys(Fmoc)-OH	Z-DL-Lys(cbz)-OH
Fmoc-Gly-Ol	Gly-Gly-Leu	H-Gly-Obzl.Tos	Boc-Trp-Gly
Fmoc-Gly-OH	Gly-Gly-Gly	Gly-Obzl	Fmoc-L-Thr(tBu)-Gly-OH
Fmoc-Gly-Val-OH	Ala-gly	Gly-Obzl.hcl	Met-Gly.HCl
Fmoc-Gly-Gly-OH	Ala-Gly-Ome.hcl	Tos-Gly-Ome	H-Met-Gly-OH
Fmoc-Gly-Gly-Gly-OH	Boc-Ala-Gly-OH	H-Gly-Oet.HCl	Cbz-D-Arg-Gly-OH
Fmoc-Gly-Gly-Gly-Gly-OH	Fmoc-Ala-gly-OH	Gly.HCL	Boc-His(Trt)-Gly-OH
H-Gly-NH2.HCl	Boc-Gly-OL

Boemo bo phahameng

1. Tshebeletso ya R&D e teng
2. Moetsi ea netefalitsoeng oa ISO, tiiso ea boleng
3.Tsamaiso e feletseng ea ts'ebeletso ea ho latela nakong ea tlhahiso
4.Chelete e phahameng e atlehang
5.Litokomane tsa setifikeiti sa boleng tse fanoeng ho latela kopo ea moreki
Tšebeletso ea 6.E kholo ka mor'a thekiso, ho boloka kamano e haufi le moreki
7.Mohloli o felletseng oa ho thusa ho fokotsa litšenyehelo tsa ho tsamaisa thepa
8.Free sampole e filwe ho hlahloba tsoa boleng pele ho tefo efe kapa efe
9.Ho buisanoa ka nako ea tefo
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